Relative Reactivity of Anilines Relative Reactivity of Anilines Abstract: several(a) Anilines were tested with Br2/HBr solution, the products were crystallized and melting points attained to verify relation reactivity. My assignment, 2,4-Dibromoanisol, was prepared in a yield of 52% with a melting point of 55-58 C . Reaction: Mechanism: outgrowth: Anisole (0.35mL, 0.0378mol) was obtained and organised in a pre-weighed 25 mL flesh out bottom flask, along with 2.5 mL of glacial acetic acid and a magnetic stir bar.
Then the reaction prickin g was assembled, the dry tube was charged with conc. sodium bi sulfate, the 25 mL round bottom was attached to the apparatus, and 5 mL of Br2/HBr mixture was obtained and pose in the round bottom. The reaction took govern for 20 minutes. An orange liquid was obtained and laid in a 125 mL Erlenmeyer flask along with 25 mL of water and 2.5 mL of conc. Sodium bisulfate soln. The solution was then placed in an ice bath...If you want to get a profound essay, order it on our website: OrderCustomPaper.com
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